Universität Wien
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270036 VO Structure-determination 1D/2D NMR (2019S)

Structure-determination using one- and two-diimensional NMR-Spectroscopy

1.50 ECTS (1.00 SWS), SPL 27 - Chemie
Moodle

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Details

Language: German

Examination dates

Lecturers

Classes (iCal) - next class is marked with N

  • Monday 06.05. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 09.05. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 13.05. 13:00 - 14:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 16.05. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 20.05. 13:00 - 14:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 23.05. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 27.05. 13:00 - 14:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 03.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 06.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 13.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 17.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Monday 24.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1
  • Thursday 27.06. 14:00 - 15:00 Seminarraum 3 Organische Chemie 1OG Boltzmanngasse 1

Information

Aims, contents and method of the course

Aims:
The students should learn to determine structures of small organic molecules in solution from 1D and 2D NMR spectra. The NMR spectra are used as part of a PowerPoint presentation and the blackboard is used.

Contents:
Determination of constitution, configuration and conformation of small organic molecules. Use of modern software for NMR spectral analysis. Interpretation of 1D NMR spectra as well as of homo- and heteronuclear 2D NMR spectra (DQF-COSY, TOCSY, HMQC, HMBC, NOESY).

Method:
The interpretation of the spectra should be carried out after an introduction by the participants independently on several examples. For this purpose, spectra are provided via Moodle. The structure explanation will be discussed afterwards in the course. Visualizations are performed by Power Point presentation.

Assessment and permitted materials

Written exam. Elucidation of the structure of a small organic molecule from the 1D and 2D NMR spectra and answering questions about it. The documents from the course can be used.
Dates for the exams will be discussed during the lecture.

Minimum requirements and assessment criteria

Minimum requirement:
25 points out of a maximum of 50 possible points in the written exam.

Rating Scale:
50.00 - 43.75 points -- Sehr Gut (Very good performance with knowledge of (almost) all methods, contexts and terminology.)
43.50 - 37.50 Points -- Gut (Certain uncertainties in dealing with the topics covered in the course.)
37.25 - 31.25 points -- Befriedigend (Average Exam.)
31,00 - 25,00 Points -- Genügend (Considerable deficits, but just acceptable handling of the topic, see "Minimum requirement.")
24,75 - 00,00 Points -- Nicht Genügend (Unacceptable handling of the topics covered in the course)

Examination topics

Documents (spectra) are provided via Moodle. A sample examination will be discussed during the course approximately one to two weeks before the first exam date.

Reading list

Documents (spectra) are provided via Moodle.

Association in the course directory

OC-5

Last modified: Mo 07.09.2020 15:41