Universität Wien
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321013 PR Drug Synthesis - Laboratory Course - B7 (2024W)

(5 Kurse)

8.00 ECTS (8.00 SWS), SPL 32 - Pharmazie
Continuous assessment of course work

Anmeldung in 2 Schritten:
1. U:Space 321013 ( https://uspace.univie.ac.at/ )
UND
2. Anmeldesystem Pharmazie ( https://spl-pharmazie.univie.ac.at/anmeldesystemPHARMAZIE/ )

Registration/Deregistration

Note: The time of your registration within the registration period has no effect on the allocation of places (no first come, first served).

Details

Language: German

Lecturers

Classes (iCal) - next class is marked with N

  • Wednesday 02.10. 16:45 - 18:15 UZA2 Hörsaal 4 (Raum 2Z221) 2.OG
  • Friday 04.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Monday 07.10. 11:30 - 13:00 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Wednesday 09.10. 16:45 - 18:15 UZA2 Hörsaal 8 (Raum 2Z206) 2.OG
  • Friday 11.10. 16:45 - 18:15 UZA2 Hörsaal 4 (Raum 2Z221) 2.OG
  • Monday 14.10. 11:30 - 13:00 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Wednesday 16.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Friday 18.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Wednesday 23.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Friday 25.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Wednesday 30.10. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Wednesday 06.11. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG
  • Friday 08.11. 16:45 - 18:15 UZA2 Hörsaal 5 (Raum 2Z202) 2.OG

Information

Aims, contents and method of the course

Glassware of a preparativ organic laboratory; weighting; adding of compounds to a reaction vessel; control of temperature; extraction techniques; distillation (at atmospheric pressure - at diminished pressure); fractional distillation; recrystallation; drying of solids and liquids; azeotropic distillation - water separation unit, adding of compounds via septum and syringe.
Program:
Distillation at normal pressure; distillation under reduced pressure; recrystallization; isolation of an organic acid or base, respectively, by extraction.
Eight syntheses: Reactions of carboxylic acids; reactions of carbonyl compounds; Aldol condensation, benzilic acid rearrangement reaction); reductions (sodium borohydride) and oxidation reactions; syntheses of heterocyclic compounds; Grignard-reactions (use of septum and syringe); preparation of drugs (nifedipine, phenytoin, paracetamol, acetylsalicylic acid).

Assessment and permitted materials

Evaluation is based on laboratory work; compulsory attendance.

Minimum requirements and assessment criteria

The objective of the course is to teach the student in experimental techniques used in organic synthesis. This is illustrated by a number of important organic reactions. Practical training is given in this laboratory course.

Examination topics

Laboratory course

Reading list

Organikum; Wiley-VCH

Association in the course directory

A202, BA13

Last modified: Mo 29.07.2024 13:26